6TUB

Beta-endorphin amyloid fibril


SOLID-STATE NMR
NMR Experiment
ExperimentTypeSample ContentsSolventIonic StrengthpHPressureTemperature (K)Spectrometer
12D CHHC2 mg/mL [U-100% 13C; U-100% 15N] beta-endorphin, 90 % H2O, 10 % [U-2H] D2O90% H2O/10% D2On.a.5.5AMBIENT Pa273Bruker AVANCE 850
22D PAR2 mg/mL [U-100% 13C; U-100% 15N] beta-endorphin, 90 % H2O, 10 % [U-2H] D2O90% H2O/10% D2On.a.5.5AMBIENT Pa273Bruker AVANCE 850
32D PDSD2 mg/mL [U-100% 13C; U-100% 15N] beta-endorphin, 90 % H2O, 10 % [U-2H] D2O90% H2O/10% D2On.a.5.5AMBIENT Pa273Bruker AVANCE 850
NMR Spectrometer Information
SpectrometerManufacturerModelField Strength
1BrukerAVANCE850
NMR Refinement
MethodDetailsSoftware
torsion angle dynamicsCYANA
NMR Ensemble Information
Conformer Selection Criteriatarget function
Conformers Calculated Total Number95
Conformers Submitted Total Number10
Representative Model1 (closest to the average)
Computation: NMR Software
#ClassificationVersionSoftware NameAuthor
1structure calculationCYANA3.98.3Guentert, P.
2chemical shift assignmentCcpNmr AnalysisCCPN