NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D NOESY | 2 mM unlabelled BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 800 |
2 | 2D TOCSY | 2 mM unlabelled BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 800 |
3 | 2D DQF-COSY | 2 mM unlabelled BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 800 |
4 | 3D HNCACB | 1 mM [U-99% 13C; U-99% 15N] BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 600 |
5 | 3D CBCA(CO)NH | 1 mM [U-99% 13C; U-99% 15N] BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 600 |
11 | 3D HNCO | 1 mM [U-99% 13C; U-99% 15N] BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 600 |
10 | 3D HNCACO | 1 mM [U-99% 13C; U-99% 15N] BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 600 |
9 | 3D HBHA(CO)NH | 1 mM [U-99% 13C; U-99% 15N] BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 600 |
8 | 2D 1H-15N HSQC | 1 mM [U-99% 13C; U-99% 15N] BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 600 |
7 | 2D 1H-13C HSQC | 1 mM [U-99% 13C; U-99% 15N] BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 600 |
6 | 2D 1H-13C HSQC aliphatic | 1 mM [U-10% 13C] BRG1 BRK domain | 90% H2O/10% D2O | 140 mM | 6.5 | 1 atm | 293 | Bruker AVANCE 600 |