NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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2 | TROSY-HSQC | 1 mM U-15N; U-13-; U-2H 15N-, 13C-, and 2H-isotopically enriched | 100% D2O | 20 mM | 6.3 | 1 bar | 293 | Bruker 900-MHz Bruker Avance-II 900 |
1 | 4D 1H-15N-15N-1H HMQC-NOESY-TROSY-HSQC | 1 mM U-15N; U-13-; U-2H 15N-, 13C-, and 2H-isotopically enriched | 100% D2O | 20 mM | 6.3 | 1 bar | 293 | Bruker 900-MHz Bruker Avance-II 900 |
3 | 3D TROSY-HNCACB | 1 mM U-15N; U-13-; U-2H 15N-, 13C-, and 2H-isotopically enriched | 100% D2O | 20 mM | 6.3 | 1 bar | 293 | Bruker 900-MHz Bruker Avance-II 900 |
4 | ARTSY-J | 1 mM U-15N; U-2H 15N-, and 2H-isotopically enriched | 100% D2O | 20 mM | 6.3 | 1 bar | 293 | Bruker 900-MHz Bruker Avance-II 900 |
5 | WEX-III TROSY | 1 mM U-15N; U-2H 15N-, and 2H-isotopically enriched | 100% D2O | 25 mM | 7.8 | 1 bar | 293 | Bruker 900-MHz Bruker Avance-II 900 |
6 | ARTSY | 1 mM U-15N; U-13-; U-2H 15N-, 13C-, and 2H-isotopically enriched | 100% D2O | 25 mM | 6.3 | 1 bar | 293 | Bruker 900-MHz Bruker Avance-II 900 |
11 | ARTSY | 1 mM U-15N; U-13-; U-2H 15N-, 13C-, and 2H-isotopically enriched | 100% D2O | 100 mM | 6.3 | 1 bar | 293 | Bruker 900-MHz Bruker Avance-II 900 |
7 | E.COSY-HSQC-TROSY | 1 mM U-15N; U-13-; U-2H 15N-, 13C-, and 2H-isotopically enriched | 100% D2O | 25 mM | 6.3 | 1 bar | 293 | Bruker 900-MHz Bruker Avance-II 900 |
8 | ARTSY | 1 mM U-15N; U-13-; U-2H I13C MT-DOTA-Lu/Tm | 100% D2O | 25 mM | 6.3 | 1 bar | 293 | Bruker 900-MHz Bruker Avance-II 900 |
9 | Heteronuclear TROSY-based relaxation | 1 mM U-15N; U-2H 15N-, and 2H-isotopically enriched | 100% D2O | 20 mM | 6.3 | 1 bar | 293 | Bruker 800-MHz Bruker 800 |
10 | Heteronuclear TROSY-based relaxation | 1 mM U-15N; U-2H 15N-, and 2H-isotopically enriched | 100% D2O | 20 mM | 6.3 | 1 bar | 293 | Bruker 600-MHz Bruker 600 |