NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-1H NOESY | 0.7 mM NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
2 | 2D 1H-1H TOCSY | 0.7 mM NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
3 | 2D 1H-1H NOESY | 0.7 mM NPHP1CC | 100% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
4 | 2D 1H-1H TOCSY | 0.7 mM NPHP1CC | 100% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
5 | 2D 1H-15N HSQC | 0.9 mM [U-99% 15N] NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
6 | 3D HNHA | 0.9 mM [U-99% 15N] NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
7 | 3D 1H-15N NOESY | 0.9 mM [U-99% 15N] NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 900 |
8 | 3D HNCA | 0.8 mM [U-99% 13C; U-99% 15N] NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
9 | 3D H(CCO)NH | 0.8 mM [U-99% 13C; U-99% 15N] NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
10 | 3D HNCACB | 0.8 mM [U-99% 13C; U-99% 15N] NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
11 | 3D CBCA(CO)NH | 0.8 mM [U-99% 13C; U-99% 15N] NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
12 | 3D C(CO)NH | 0.8 mM [U-99% 13C; U-99% 15N] NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
13 | 3D HNCO | 0.8 mM [U-99% 13C; U-99% 15N] NPHP1CC | 90% H2O/10% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 600 |
14 | 3D HCCH-TOCSY | 0.8 mM [U-99% 13C; U-99% 15N] NPHP1 CC | 100% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 900 |
15 | 2D 1H-13C HSQC | 0.8 mM [U-99% 13C; U-99% 15N] NPHP1 CC | 100% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 900 |
16 | 3D 1H-13C NOESY | 0.8 mM [U-99% 13C; U-99% 15N] NPHP1 CC | 100% D2O | 0.15 M | 6.3 | ambient | 298 | Bruker AVANCE 900 |