NMR Experiment |
---|
Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
---|
1 | 2D 1H-15N HSQC | 1 mM [U-13C;15N] gHEEE_02, 5 uM DSS, 0.02 % sodium azide | 90% H2O/10% D2O | 50 mM | 6.0 | ambient | 298 | Varian INOVA 750 |
2 | 2D 1H-13C HSQC aliphatic | 1 mM [U-13C;15N] gHEEE_02, 5 uM DSS, 0.02 % sodium azide | 90% H2O/10% D2O | 50 mM | 6.0 | ambient | 298 | Varian INOVA 750 |
3 | 2D 1H-13C HSQC aromatic | 1 mM [U-13C;15N] gHEEE_02, 5 uM DSS, 0.02 % sodium azide | 90% H2O/10% D2O | 50 mM | 6.0 | ambient | 298 | Varian INOVA 750 |
4 | 3D HNCO | 1 mM [U-13C;15N] gHEEE_02, 5 uM DSS, 0.02 % sodium azide | 90% H2O/10% D2O | 50 mM | 6.0 | ambient | 298 | Varian INOVA 750 |
5 | 3D CBCA(CO)NH | 1 mM [U-13C;15N] gHEEE_02, 5 uM DSS, 0.02 % sodium azide | 90% H2O/10% D2O | 50 mM | 6.0 | ambient | 298 | Varian INOVA 750 |
10 | 3D HNCACB | 1 mM [U-13C;15N] gHEEE_02, 5 uM DSS, 0.02 % sodium azide | 90% H2O/10% D2O | 50 mM | 6.0 | ambient | 298 | Varian INOVA 750 |
9 | 3D HBHA(CO)NH | 1 mM [U-13C;15N] gHEEE_02, 5 uM DSS, 0.02 % sodium azide | 90% H2O/10% D2O | 50 mM | 6.0 | ambient | 298 | Varian INOVA 750 |
8 | 3D HCCH-TOCSY | 1 mM [U-13C;15N] gHEEE_02, 5 uM DSS, 0.02 % sodium azide | 90% H2O/10% D2O | 50 mM | 6.0 | ambient | 298 | Varian INOVA 750 |
7 | GFT 4,3D HCCH-COSY | 1 mM [U-13C;15N] gHEEE_02, 5 uM DSS, 0.02 % sodium azide | 90% H2O/10% D2O | 50 mM | 6.0 | ambient | 298 | Varian INOVA 750 |
6 | 3D 15N/13Caliphatic/13Caromatic-edited [1H,1H]-NOESY | 1 mM [U-13C;15N] gHEEE_02, 5 uM DSS, 0.02 % sodium azide | 90% H2O/10% D2O | 50 mM | 6.0 | ambient | 298 | Varian INOVA 750 |