NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-1H TOCSY | 1 mM [U-99% 13C; U-99% 15N] CbnX, 50 % [U-99% 2H] trifluoroethanol, 50 % water, 0.01 % DSS | trifluoroethanol/water | 0 | 6 | 760 mmHg | 300 | Varian VNMRS 700 |
2 | 2D 1H-1H NOESY | 1 mM [U-99% 13C; U-99% 15N] CbnX, 50 % [U-99% 2H] trifluoroethanol, 50 % water, 0.01 % DSS | trifluoroethanol/water | 0 | 6 | 760 mmHg | 300 | Varian VNMRS 700 |
3 | 2D 1H-15N HSQC | 1 mM [U-99% 13C; U-99% 15N] CbnX, 50 % [U-99% 2H] trifluoroethanol, 50 % water, 0.01 % DSS | trifluoroethanol/water | 0 | 6 | 760 mmHg | 300 | Varian VNMRS 700 |
4 | 2D 1H-13C HSQC | 1 mM [U-99% 13C; U-99% 15N] CbnX, 50 % [U-99% 2H] trifluoroethanol, 50 % water, 0.01 % DSS | trifluoroethanol/water | 0 | 6 | 760 mmHg | 300 | Varian VNMRS 700 |
5 | 3D HCCH-TOCSY | 1 mM [U-99% 13C; U-99% 15N] CbnX, 50 % [U-99% 2H] trifluoroethanol, 50 % water, 0.01 % DSS | trifluoroethanol/water | 0 | 6 | 760 mmHg | 300 | Varian VNMRS 700 |
6 | 3D 1H-15N NOESY | 1 mM [U-99% 13C; U-99% 15N] CbnX, 50 % [U-99% 2H] trifluoroethanol, 50 % water, 0.01 % DSS | trifluoroethanol/water | 0 | 6 | 760 mmHg | 300 | Varian VNMRS 700 |
7 | 3D 1H-15N TOCSY | 1 mM [U-99% 13C; U-99% 15N] CbnX, 50 % [U-99% 2H] trifluoroethanol, 50 % water, 0.01 % DSS | trifluoroethanol/water | 0 | 6 | 760 mmHg | 300 | Varian VNMRS 700 |