NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
2 | 3D HNCO | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
3 | 3D HN(CA)CO | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
4 | 3D CBCA(CO)NH | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
5 | 3D HNCACB | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
6 | 3D C(CO)NH | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
7 | 3D HBHA(CO)NH | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
8 | 2D 1H-13C HSQC | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
9 | 3D HCCH-TOCSY | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
10 | 3D HCCH-COSY | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
11 | 3D 1H-15N NOESY | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |
12 | 3D 1H-13C NOESY | 0.4 mM [U-100% 13C; U-100% 15N] entity-1, 20 mM sodium phosphate-2, 150 mM sodium chloride-3, 1 mM DTT-4 | 95% H2O/5% D2O | 170 | 7.0 | ambient | 298 | |