NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
2 | 2D 1H-13C HSQC aliphatic | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
3 | 2D 1H-13C HSQC aromatic | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
4 | 3D HNCO | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
5 | 3D HNCA | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
6 | 3D HNCACB | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
7 | 3D HN(CO)CA | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
8 | 3D HN(CA)CO | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
9 | 3D CBCA(CO)NH | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
10 | 3D HBHA(CO)NH | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
11 | 3D HCCH-COSY | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
12 | 3D HCCH-TOCSY | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
13 | 3D 1H-15N NOESY | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
14 | 3D 1H-13C NOESY aliphatic | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
15 | 3D 1H-13C NOESY aromatic | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
16 | 3D 13C/15N filtered NOESY | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
17 | 2D 13C/15N fllterd NOESY | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |
18 | 2D 13C/15N filterd TOCSY | 0.3-0.5mM [U-99% 13C; U-99% 15N] Chp1_chromodomain-1, 0.3-0.5mM Histone_H3K9me3-2, 20mM potassium phosphate-3, 10mM sodium chloride-4 | 90% H2O/10% D2O | | 6.8 | ambient | 298 | |