NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 1 mM [U-100% 15N] Blo t 19-4, 50 mM potassium phosphate-5, 100 mM sodium chloride-6 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
2 | 2D 1H-13C HSQC | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
3 | 3D HNCO | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
4 | 3D HN(CA)CO | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
5 | 3D HNCA | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
6 | 3D HNCACB | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
7 | 3D CBCA(CO)NH | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
8 | 3D HNHA | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
9 | 3D HCCH-COSY | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
10 | 3D HCCH-TOCSY | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
11 | 2D-hbCBcgcdHD | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
12 | 2D-hbCBcgcdceHE | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
13 | 2D-TOCSY | 1 mM Blo t 19-7, 50 mM potassium phosphate-8, 100 mM sodium chloride-9 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
14 | 3D 1H-15N TOCSY | 1 mM [U-100% 15N] Blo t 19-4, 50 mM potassium phosphate-5, 100 mM sodium chloride-6 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
15 | 2D 1H-1H NOESY | 1 mM Blo t 19-7, 50 mM potassium phosphate-8, 100 mM sodium chloride-9 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
16 | 3D 1H-13C NOESYHSQC | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
17 | 3D 1H-15N NOESYHSQC | 1 mM [U-100% 13C; U-100% 15N] Blo t 19-1, 50 mM potassium phosphate-2, 100 mM sodium chloride-3 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |
18 | 2D 1H-15N IPAP HSQC | 1 mM [U-100% 15N] Blo t 19-10, 50 mM potassium phosphate-11, 100 mM sodium chloride-12, 15 mg/ml Pf1 phage-13 | 90% H2O/10% D2O | | 6.0 | ambient | 295 | |