NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 1 mM [U-15N] Holo ACPI, 5 % D2O, 0.15 mM DSS, 50 mM Arginine, 50 mM Glutamate | 95% H2O/5% D2O | | 6.8 | ambient | 291 | |
2 | 3D HNCACB | 1 mM [U-15N],[U-13C] Holo ACPI, 5 % D2O, 0.15 mM DSS, 50 mM Arginine, 50 mM Glutamate | 95% H2O/5% D2O | | 6.8 | ambient | 291 | |
3 | 3D HNCO | 1 mM [U-15N],[U-13C] Holo ACPI, 5 % D2O, 0.15 mM DSS, 50 mM Arginine, 50 mM Glutamate | 95% H2O/5% D2O | | 6.8 | ambient | 291 | |
4 | 3D HNCACO | 1 mM [U-15N],[U-13C] Holo ACPI, 5 % D2O, 0.15 mM DSS, 50 mM Arginine, 50 mM Glutamate | 95% H2O/5% D2O | | 6.8 | ambient | 291 | |
5 | 3D H(CCCO)NH-TOCSY | 1 mM [U-15N],[U-13C] Holo ACPI, 5 % D2O, 0.15 mM DSS, 50 mM Arginine, 50 mM Glutamate | 95% H2O/5% D2O | | 6.8 | ambient | 291 | |
6 | 3D (H)C(CCO)NH-TOCSY | 1 mM [U-15N],[U-13C] Holo ACPI, 5 % D2O, 0.15 mM DSS, 50 mM Arginine, 50 mM Glutamate | 95% H2O/5% D2O | | 6.8 | ambient | 291 | |
7 | 3D 1H-13C NOESY | 1 mM [U-15N] Holo ACPI, 5 % D2O, 0.15 mM DSS, 50 mM Arginine, 50 mM Glutamate | 95% H2O/5% D2O | | 6.8 | ambient | 291 | |
8 | 3D 1H-15N NOESY | 1 mM [U-13C] Holo ACPI, 5 % D2O, 0.15 mM DSS, 50 mM Arginine, 50 mM Glutamate | 95% H2O/5% D2O | | 6.8 | ambient | 291 | |
9 | (H)CB(CGCC-TOCSY)Har | 1 mM [U-15N],[U-13C] Holo ACPI, 5 % D2O, 0.15 mM DSS, 50 mM Arginine, 50 mM Glutamate | 95% H2O/5% D2O | | 6.8 | ambient | 291 | |