NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 0.55 mM [U-100% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
2 | 2D 1H-13C HSQC | 0.55 mM [U-100% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
3 | 3D HNCO | 0.55 mM [U-100% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
4 | 3D CBCA(CO)NH | 0.55 mM [U-100% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
5 | 3D HNCACB | 0.55 mM [U-100% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
6 | 3D HBHA(CO)NH | 0.55 mM [U-100% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
7 | 3D simutaneous 13C-aromatic,13C-aliphatic,15N edited 1H-1H NOESY | 0.55 mM [U-100% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
8 | 2D 1H-15N HSQC | 0.55 mM [U-5% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS, 13 mg/mL Pf1 phage | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
9 | 2D 1H-13C HSQC | 0.55 mM [U-5% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
10 | 3D HCCH-TOCSY | 0.55 mM [U-100% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
11 | 3D HCCH-COSY | 0.55 mM [U-100% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |
12 | HB(CBCGCDCE)HE | 0.55 mM [U-100% 13C; U-100% 15N] MaR143A, 100 mM sodium chloride, 5 mM DTT, 0.02 % sodium azide, 10 mM TRIS | 95% H2O/5% D2O | | 7.5 | ambient | 298 | |