NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 1mM [U-100% 15N] PC1/3 DCSG-sorting domain-1, 1mM [U-100% 13C; U-100% 15N] PC1/3 DCSG-sorting domain-2 | 90% H2O/10% D2O | | 6.5 | ambient | 300 | |
2 | 3D HNCO | 1mM [U-100% 15N] PC1/3 DCSG-sorting domain-1, 1mM [U-100% 13C; U-100% 15N] PC1/3 DCSG-sorting domain-2 | 90% H2O/10% D2O | | 6.5 | ambient | 300 | |
3 | 3D HNCA | 1mM [U-100% 15N] PC1/3 DCSG-sorting domain-1, 1mM [U-100% 13C; U-100% 15N] PC1/3 DCSG-sorting domain-2 | 90% H2O/10% D2O | | 6.5 | ambient | 300 | |
4 | 3D HNCACB | 1mM [U-100% 15N] PC1/3 DCSG-sorting domain-1, 1mM [U-100% 13C; U-100% 15N] PC1/3 DCSG-sorting domain-2 | 90% H2O/10% D2O | | 6.5 | ambient | 300 | |
5 | 3D HBHA(CO)NH | 1mM [U-100% 15N] PC1/3 DCSG-sorting domain-1, 1mM [U-100% 13C; U-100% 15N] PC1/3 DCSG-sorting domain-2 | 90% H2O/10% D2O | | 6.5 | ambient | 300 | |
6 | 3D HN(CO)CA | 1mM [U-100% 15N] PC1/3 DCSG-sorting domain-1, 1mM [U-100% 13C; U-100% 15N] PC1/3 DCSG-sorting domain-2 | 90% H2O/10% D2O | | 6.5 | ambient | 300 | |
7 | 3D HCCH-TOCSY | 1mM [U-100% 15N] PC1/3 DCSG-sorting domain-1, 1mM [U-100% 13C; U-100% 15N] PC1/3 DCSG-sorting domain-2 | 90% H2O/10% D2O | | 6.5 | ambient | 300 | |
8 | 3D 1H-15N NOESY | 1mM [U-100% 15N] PC1/3 DCSG-sorting domain-1, 1mM [U-100% 13C; U-100% 15N] PC1/3 DCSG-sorting domain-2 | 90% H2O/10% D2O | | 6.5 | ambient | 300 | |
9 | 3D 1H-13C NOESY | 1mM [U-100% 15N] PC1/3 DCSG-sorting domain-1, 1mM [U-100% 13C; U-100% 15N] PC1/3 DCSG-sorting domain-2 | 90% H2O/10% D2O | | 6.5 | ambient | 300 | |