NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
2 | 2D 1H-13C HSQC | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
3 | 3D CBCA(CO)NH | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
4 | 3D C(CO)NH | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
5 | 3D HNCO | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
6 | 3D HNCACB | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
7 | 3D HN(CO)CA | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
8 | 3D H(CCO)NH | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
9 | 3D HCCH-TOCSY | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
10 | 3D HCCH-COSY | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
11 | 3D 1H-15N NOESY | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
12 | 3D 1H-13C NOESY | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
13 | 3D iHNCA | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
14 | 3D 1H-13C NOESY (AROM) | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
15 | (H )C (C C )H | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
16 | (H )C (C C C )H | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
17 | J(CN) intensity modulated constant time 13C-HSQC | 1 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
18 | 3D R1 resolved 1H-15N-HSQC | 0.3 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
19 | 3D R2 resolved 1H-15N-HSQC | 0.3 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |
20 | exchange rate resolved 1H-15N-HSQC | 0.3 mM [U-15N] PrsA-PPIase, 20 mM Bis-TRIS, 1 mM sodium azide, 1 mM EDTA | 92% H2O/8% D2O | 20 | 6.8 | ambient | 298 | |