2IXY

Solution structure of the apical stem-loop of the human hepatitis B virus encapsidation signal

SOLUTION NMR

NMR Experiment
Experiment	Type	Sample Contents	Solvent	Ionic Strength	pH	Pressure	Temperature (K)	Spectrometer
1	NOESY	D2O, 10% D2O/90% H2O		100	7.0	1.0 atm	298.0
2	COSY	D2O, 10% D2O/90% H2O		100	7.0	1.0 atm	298.0
3	TOCSY	D2O, 10% D2O/90% H2O		100	7.0	1.0 atm	298.0
4	HSQC	D2O, 10% D2O/90% H2O		100	7.0	1.0 atm	298.0

NMR Spectrometer Information
Spectrometer	Manufacturer	Model	Field Strength
1	Bruker	DRX	600

NMR Refinement
Method	Details	Software
simulated annealing	REFINEMENT DETAILS CAN BE FOUND IN THE JRNL CITATION ABOVE	X-PLOR

NMR Ensemble Information
Conformer Selection Criteria
Conformers Calculated Total Number	100
Conformers Submitted Total Number	23

Additional NMR Experimental Information
Details	NONE

Computation: NMR Software
#	Classification	Version	Software Name	Author
1	refinement	X-PLOR		BRUNGER
2	structure solution	X-PLOR

RCSB PDB Core Operations are funded by the National Science Foundation (DBI-1832184), the US Department of Energy (DE-SC0019749), and the National Cancer Institute, National Institute of Allergy and Infectious Diseases, and National Institute of General Medical Sciences of the National Institutes of Health under grant R01GM133198.