1VYX

Solution structure of the KSHV K3 N-terminal domain


SOLUTION NMR
NMR Experiment
ExperimentTypeSample ContentsSolventIonic StrengthpHPressureTemperature (K)Spectrometer
1NOESY50 MM POTASSIUM PHOSPHATE (PH 6.0), CONTAINING 50 MM NACL100.0 mM6.0ambient atm298.0
2TOCSY50 MM POTASSIUM PHOSPHATE (PH 6.0), CONTAINING 50 MM NACL100.0 mM6.0ambient atm298.0
3DQF-COSY50 MM POTASSIUM PHOSPHATE (PH 6.0), CONTAINING 50 MM NACL100.0 mM6.0ambient atm298.0
4HNCACB50 MM POTASSIUM PHOSPHATE (PH 6.0), CONTAINING 50 MM NACL100.0 mM6.0ambient atm298.0
5CBCACONH50 MM POTASSIUM PHOSPHATE (PH 6.0), CONTAINING 50 MM NACL100.0 mM6.0ambient atm298.0
6HNCO50 MM POTASSIUM PHOSPHATE (PH 6.0), CONTAINING 50 MM NACL100.0 mM6.0ambient atm298.0
7HNCACO50 MM POTASSIUM PHOSPHATE (PH 6.0), CONTAINING 50 MM NACL100.0 mM6.0ambient atm298.0
813C-HSQC50 MM POTASSIUM PHOSPHATE (PH 6.0), CONTAINING 50 MM NACL100.0 mM6.0ambient atm298.0
9HNHB50 MM POTASSIUM PHOSPHATE (PH 6.0), CONTAINING 50 MM NACL100.0 mM6.0ambient atm298.0
NMR Spectrometer Information
SpectrometerManufacturerModelField Strength
1BrukerAVANCE800
NMR Refinement
MethodDetailsSoftware
XPLOR3.8REFINEMENT DETAILS CAN BE FOUND IN THE JRNL CITATION ABOVEX-PLOR
NMR Ensemble Information
Conformer Selection CriteriaNO VIOLATIONS GREATER THAN 0.25A, NO ANGLE VIOLATIONS
Conformers Calculated Total Number30
Conformers Submitted Total Number28
Representative Model1 (n/a)
Additional NMR Experimental Information
DetailsTHE STRUCTURE WAS DETERMINED USING STANDAR TRIPLE- RESONANCE METHODS ON 13C-15N-LABELLED K3-RING DOMAIN
Computation: NMR Software
#ClassificationVersionSoftware NameAuthor
1refinementX-PLORBRUNGER
2structure solutionXwinNMR
3structure solutionANSIG
4structure solutionX-PLOR