NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D NOESY | 1.1MM APO-CCME-H6 U-98% 13C; U-98% 15N; 50MM PHOSPHATE BUFFER, PH 7.2, 300MM NACL, 90% H2O, 10% D2O | 90% H2O/10% D2O | | 7.2 | AMBIENT | 303 | |
2 | 2D TOCSY | 1.1MM APO-CCME-H6 U-98% 13C; U-98% 15N; 50MM PHOSPHATE BUFFER, PH 7.2, 300MM NACL, 90% H2O, 10% D2O | 90% H2O/10% D2O | | 7.2 | AMBIENT | 303 | |
3 | 3D_13C- SEPARATED_NOESY | 1.1MM APO-CCME-H6 U-98% 13C; U-98% 15N; 50MM PHOSPHATE BUFFER, PH 7.2, 300MM NACL, 90% H2O, 10% D2O | 90% H2O/10% D2O | | 7.2 | AMBIENT | 303 | |
4 | 3D_15N- SEPARATED_NOESY | 1.1MM APO-CCME-H6 U-98% 13C; U-98% 15N; 50MM PHOSPHATE BUFFER, PH 7.2, 300MM NACL, 90% H2O, 10% D2O | 90% H2O/10% D2O | | 7.2 | AMBIENT | 303 | |
5 | 2D_TROSY | 1.1MM APO-CCME-H6 U-98% 13C; U-98% 15N; 50MM PHOSPHATE BUFFER, PH 7.2, 300MM NACL, 90% H2O, 10% D2O | 90% H2O/10% D2O | | 7.2 | AMBIENT | 303 | |
6 | 3D_ TROSY_HNCA | 1.1MM APO-CCME-H6 U-98% 13C; U-98% 15N; 50MM PHOSPHATE BUFFER, PH 7.2, 300MM NACL, 90% H2O, 10% D2O | 90% H2O/10% D2O | | 7.2 | AMBIENT | 303 | |
7 | 3D_TROSY_HNCACB | 1.1MM APO-CCME-H6 U-98% 13C; U-98% 15N; 50MM PHOSPHATE BUFFER, PH 7.2, 300MM NACL, 90% H2O, 10% D2O | 90% H2O/10% D2O | | 7.2 | AMBIENT | 303 | |
8 | CBCA(CO)NH | 1.1MM APO-CCME-H6 U-98% 13C; U-98% 15N; 50MM PHOSPHATE BUFFER, PH 7.2, 300MM NACL, 90% H2O, 10% D2O | 90% H2O/10% D2O | | 7.2 | AMBIENT | 303 | |
9 | HCCH-TOCSA | 1.1MM APO-CCME-H6 U-98% 13C; U-98% 15N; 50MM PHOSPHATE BUFFER, PH 7.2, 300MM NACL, 90% H2O, 10% D2O | 90% H2O/10% D2O | | 7.2 | AMBIENT | 303 | |
10 | 15N_ EDITED_TOCSY | 1.1MM APO-CCME-H6 U-98% 13C; U-98% 15N; 50MM PHOSPHATE BUFFER, PH 7.2, 300MM NACL, 90% H2O, 10% D2O | 90% H2O/10% D2O | | 7.2 | AMBIENT | 303 | |