Experiment: 1OVQ

SOLUTION NMR

NMR Experiment
Experiment	Type	Sample Contents	Solvent	Ionic Strength	pH	Pressure	Temperature (K)	Spectrometer
1	3D_15N-separated_NOESY	U-15N,13C; 75 mM KiPO4, pH 7.5, 5 mM DTT	95% H2O/5% D2O	0.45	7.5	ambient	298
2	3D_13C-separated_NOESY	U-15N,13C; 75 mM KiPO4, pH 7.5, 5 mM DTT	95% H2O/5% D2O	0.45	7.5	ambient	298
3	3D_13C-separated_NOESY	U-15N,13C; 75 mM KiPO4, pH 7.5, 5 mM DTT	99%D2O	0.45	7.5	ambient	298

NMR Spectrometer Information
Spectrometer	Manufacturer	Model	Field Strength
1	Varian	INOVA	600

NMR Refinement
Method	Details	Software
simulated annealing		X-PLOR

NMR Ensemble Information
Conformer Selection Criteria	back calculated data agree with experimental NOESY spectrum
Conformers Calculated Total Number	100
Conformers Submitted Total Number	25

Computation: NMR Software
#	Classification	Version	Software Name	Author
1	structure solution	X-PLOR	98	msi
2	processing	Felix	98	msi
3	refinement	X-PLOR	98	msi

RCSB PDB Core Operations are funded by the National Science Foundation (DBI-1832184), the US Department of Energy (DE-SC0019749), and the National Cancer Institute, National Institute of Allergy and Infectious Diseases, and National Institute of General Medical Sciences of the National Institutes of Health under grant R01GM133198.