1OCI
[3.2.0]bcANA:DNA
SOLUTION NMR
| NMR Experiment | ||||||||
|---|---|---|---|---|---|---|---|---|
| Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
| 1 | STANDARD 2D NMR EXPERIMENTS | 2mM NUCLEIC ACID | 10MM SODIUM PHOSPHATE BUFFER,100MM NACL mM | 7.0 | 1 atm | 298 | ||
| NMR Spectrometer Information | |||
|---|---|---|---|
| Spectrometer | Manufacturer | Model | Field Strength |
| 1 | Varian | UNITY | 500 |
| 2 | Varian | INOVA | 800 |
| NMR Refinement | ||
|---|---|---|
| Method | Details | Software |
| simulated annealing | REFINEMENT DETAILS CAN BE FOUND IN THE JRNL CITATION ABOVE. | AMBER5 |
| NMR Ensemble Information | |
|---|---|
| Conformer Selection Criteria | |
| Conformers Calculated Total Number | 40 |
| Conformers Submitted Total Number | 40 |
| Representative Model | 6 (n/a) |
| Additional NMR Experimental Information | |
|---|---|
| Details | SEE JOURNAL CITATION FOR FULL DETAILS |
| Computation: NMR Software | ||||
|---|---|---|---|---|
| # | Classification | Version | Software Name | Author |
| 1 | refinement | AMBER5 | CASE, KOLLMAN ET AL | |
| 2 | structure solution | MARDIGRAS | ||
| 3 | structure solution | AMBER | ||
