1BCV
SYNTHETIC PEPTIDE CORRESPONDING TO THE MAJOR IMMUNOGEN SITE OF FMD VIRUS, NMR, 10 STRUCTURES
SOLUTION NMR
| NMR Experiment | ||||||||
|---|---|---|---|---|---|---|---|---|
| Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
| 1 | COSY | H2O | 0.1M PHOSPHATE | 5.7 | 1 atm | 285 | ||
| 2 | TOCSY | H2O | 0.1M PHOSPHATE | 5.7 | 1 atm | 285 | ||
| 3 | ROESY | H2O | 0.1M PHOSPHATE | 5.7 | 1 atm | 285 | ||
| 4 | NOESY | H2O | 0.1M PHOSPHATE | 5.7 | 1 atm | 285 | ||
| NMR Spectrometer Information | |||
|---|---|---|---|
| Spectrometer | Manufacturer | Model | Field Strength |
| 1 | Bruker | DRX400 | 400 |
| NMR Refinement | ||
|---|---|---|
| Method | Details | Software |
| torsion angle dynamics | RESTRAINED ENERGY REFINEMENT. | DYANA |
| NMR Ensemble Information | |
|---|---|
| Conformer Selection Criteria | target function |
| Conformers Calculated Total Number | 50 |
| Conformers Submitted Total Number | 10 |
| Computation: NMR Software | ||||
|---|---|---|---|---|
| # | Classification | Version | Software Name | Author |
| 1 | refinement | DYANA | 1.4 | GUNTERT,WUTHRICH |
| 2 | structure solution | DYANA-1.4 | ||
