1A6X
STRUCTURE OF THE APO-BIOTIN CARBOXYL CARRIER PROTEIN (APO-BCCP87) OF ESCHERICHIA COLI ACETYL-COA CARBOXYLASE, NMR, 49 STRUCTURES
SOLUTION NMR
| NMR Experiment | ||||||||
|---|---|---|---|---|---|---|---|---|
| Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
| 1 | NOESY | PHOSPHATE BUFFER | 7.5 | 298 | ||||
| 2 | TOCSY | PHOSPHATE BUFFER | 7.5 | 298 | ||||
| 3 | COSY | PHOSPHATE BUFFER | 7.5 | 298 | ||||
| 4 | HSQC | PHOSPHATE BUFFER | 7.5 | 298 | ||||
| 5 | NOESY-HSQC | PHOSPHATE BUFFER | 7.5 | 298 | ||||
| 6 | TOCSY-HSQC AND T1 | PHOSPHATE BUFFER | 7.5 | 298 | ||||
| 7 | T2 | PHOSPHATE BUFFER | 7.5 | 298 | ||||
| 8 | NOE MEASUREMENTS | PHOSPHATE BUFFER | 7.5 | 298 | ||||
| NMR Spectrometer Information | |||
|---|---|---|---|
| Spectrometer | Manufacturer | Model | Field Strength |
| 1 | GE | GE OMEGA PSG | 600 |
| NMR Refinement | ||
|---|---|---|
| Method | Details | Software |
| distance geometry | REFINEMENT DETAILS CAN BE FOUND IN THE JRNL CITATION ABOVE. | DIANA |
| NMR Ensemble Information | |
|---|---|
| Conformer Selection Criteria | LEAST RESTRAINT VIOLATION |
| Conformers Calculated Total Number | 49 |
| Conformers Submitted Total Number | 49 |
| Computation: NMR Software | ||||
|---|---|---|---|---|
| # | Classification | Version | Software Name | Author |
| 1 | refinement | DIANA | GUNTERT,WUTHRICH | |
| 2 | structure solution | DIANA | ||
