NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
2 | 3D HNCO | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
3 | 3D HN(CA)CO | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
4 | 3D HNCA | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
5 | 3D HN(CO)CA | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
6 | 3D HNCACB | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
7 | 3D CBCA(CO)NH | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
8 | 3D C(CO)NH | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
9 | 3D HBHA(CO)NH | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
10 | 3D HBHANH | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
11 | 3D H(CCO)NH | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
12 | 3D 1H-15N NOESY | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
13 | 3D 1H-13C NOESY aliphatic | 913 uM [U-99% 13C; U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1.0 atm | 298 | Bruker AVANCE III 800 |
14 | 2D 1H-15N HSQC | 142 uM [U-99% 15N] Polar organizing protein Z, 5.4% acrylamide gel with 5.4 mm outer diameter (OD),95% H2O/5% D2O | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1 atm | 298 | Bruker AVANCE III 800 |
15 | 2D 1H-15N HSQC | 142 uM [U-99% 15N] Polar organizing protein Z, 5.4% acrylamide gel with 6.0 mm outer diameter | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1 atm | 298 | Bruker AVANCE III 800 |
16 | 2D 1H-15N HSQC | 142 uM [U-99% 15N] Polar organizing protein Z | 95% H2O/5% D2O | 20 mM NaCl | 5.5 | 1 atm | 298 | Bruker AVANCE III 800 |