NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
2 | 3D CBCA(CO)NH | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
3 | 3D C(CO)NH | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
4 | 3D HNCA | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
5 | 3D HNCACB | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
6 | 3D H(CCO)NH | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
7 | 3D HCCH-TOCSY | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
8 | 3D HNHA | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
9 | 3D 1H-15N NOESY | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
10 | 3D 1H-15N TOCSY | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
11 | 3D 1H-13C NOESY aliphatic | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
12 | 3D HCCH-COSY | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
13 | 3D HCACO | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |
14 | 3D HNCO | 20 mM sodium phosphate, 200 mM sodium chloride, 1 mM DTT | 90% H2O/10% D2O | 0.2 | 6.0 | ambient | 298 | |