NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 93% H2O/7% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
2 | 3D HNCA | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 93% H2O/7% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
3 | 3D HN(CO)CA | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 93% H2O/7% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
4 | 3D HNCACB | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 93% H2O/7% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
5 | 3D HCCH-TOCSY | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 100% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
6 | 3D HNCO | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 93% H2O/7% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
7 | 3D HN(CA)CO | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 93% H2O/7% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
8 | 3D 1H-15N NOESY | 0.5 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 93% H2O/7% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
9 | 3D 1H-13C NOESY | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 100% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
10 | 2D 1H-13C HSQC | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 100% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
11 | 3D CCH-TOCSY | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 100% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
12 | 3D HCCH-TOCSY aromatic | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 100% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |
13 | 2D 1H-1H NOESY | 0.2 mM [U-99% 13C; U-99% 15N] S1F1, 25.0 mM potassium phosphate, 200.0 mM potassium chloride | 100% D2O | 0.200 | 6.500 | 1.000 atm | 293.000 | |