NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 50 mM sodium phosphate, 300 mM sodium chloride, 1 mM [U-100% 15N] protein, DSS | 90% H2O/10% D2O | 0.35 | 7.5 | ambient | 296 | |
2 | 3D HNCO | 50 mM sodium phosphate, 300 mM sodium chloride, 1 mM [U-100% 13C; U-100% 15N] protein, DSS | 90% H2O/10% D2O | 0.35 | 7.5 | ambient | 296 | |
3 | CBCANH | 50 mM sodium phosphate, 300 mM sodium chloride, 1 mM [U-100% 13C; U-100% 15N] protein, DSS | 90% H2O/10% D2O | 0.35 | 7.5 | ambient | 296 | |
4 | CBCACONH | 50 mM sodium phosphate, 300 mM sodium chloride, 1 mM [U-100% 13C; U-100% 15N] protein, DSS | 90% H2O/10% D2O | 0.35 | 7.5 | ambient | 296 | |
5 | HCCCONH | 50 mM sodium phosphate, 300 mM sodium chloride, 1 mM [U-100% 13C; U-100% 15N] protein, DSS | 90% H2O/10% D2O | 0.35 | 7.5 | ambient | 296 | |
6 | CCCONH | 50 mM sodium phosphate, 300 mM sodium chloride, 1 mM [U-100% 13C; U-100% 15N] protein, DSS | 90% H2O/10% D2O | 0.35 | 7.5 | ambient | 296 | |
7 | 2D 1H-1H NOESY | 50 mM sodium phosphate, 300 mM sodium chloride, 1 mM [U-100% 15N] protein, DSS | 90% H2O/10% D2O | 0.35 | 7.5 | ambient | 296 | |
8 | 3D 1H-15N NOESY | 50 mM sodium phosphate, 300 mM sodium chloride, 1 mM [U-100% 15N] protein, DSS | 90% H2O/10% D2O | 0.35 | 7.5 | ambient | 296 | |
9 | 3D 1H-13C NOESY | 50 mM sodium phosphate, 300 mM sodium chloride, 1 mM [U-100% 13C; U-100% 15N] protein, DSS | 90% H2O/10% D2O | 0.35 | 7.5 | ambient | 296 | |