NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
2 | 2D 1H-13C HSQC | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
3 | 2D 1H-1H NOESY | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
4 | 3D HNCACB | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
5 | 3D HNCA | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
6 | 3D HNCO | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
7 | 3D HN(CA)CO | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
8 | 3D HN(COCA)CB | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
9 | 3D HCCCONH TOCSY | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
10 | 3D HBHA(CO)NH | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
11 | 3D HCCH-TOCSY | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
12 | 2D (HB)CB(CGCD)HD | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
13 | 2D (HB)CB(CGCDCE)HE | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
14 | 3D 1H-13C NOESYHSQC | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |
15 | 3D 1H-15N NOESYHSQC | 0.6mM [U-98% 13C; U-98% 15N] SQAPI-1 | 90% H2O/10% D2O | | 3 | ambient | 323 | |