NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D 1H-15N HSQC | 1mM [U-13C; U-15N] protein, 2mM protein | 90% H2O/10% D2O | 0.05 | 5.0 | ambient | 298 | |
2 | 2D 1H-13C HSQC | 1mM [U-13C; U-15N] protein, 2mM protein | 90% H2O/10% D2O | 0.05 | 5.0 | ambient | 298 | |
3 | 3D HNCO | 1mM [U-13C; U-15N] protein, 2mM protein | 90% H2O/10% D2O | 0.05 | 5.0 | ambient | 298 | |
4 | 3D HNCA | 1mM [U-13C; U-15N] protein, 2mM protein | 90% H2O/10% D2O | 0.05 | 5.0 | ambient | 298 | |
5 | 3D HNCACB | 1mM [U-13C; U-15N] protein, 2mM protein | 90% H2O/10% D2O | 0.05 | 5.0 | ambient | 298 | |
6 | 3D HCCH-TOCSY | 1mM [U-13C; U-15N] protein, 2mM protein | 90% H2O/10% D2O | 0.05 | 5.0 | ambient | 298 | |
7 | 2D 1H-1H NOESY | 1mM [U-13C; U-15N] protein, 2mM protein | 90% H2O/10% D2O | 0.05 | 5.0 | ambient | 298 | |
8 | 2D 1H-1H TOCSY | 1mM [U-13C; U-15N] protein, 2mM protein | 90% H2O/10% D2O | 0.05 | 5.0 | ambient | 298 | |