NMR Experiment |
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Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
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1 | 2D NOESY | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |
2 | 2D 15N-HSQC | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |
3 | 2D 13C-HSQC | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |
4 | 2D DQF-COSY | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |
5 | 2D HNN-COSY | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |
6 | 2D TOSCY | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |
7 | 2D 1H-31P COSY | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |
8 | 2D 15N-IPAP-HSQC | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |
9 | 3D HCCH-TOCSY | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |
10 | 3D HCCH-COSY | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |
11 | 3D 13C-SEPARATED NOESY | 2 mM [U-13C; U-15N] RNA, 10 mM sodium phosphate, 20 mM NaCl | 95% H2O/5% D2O | 20 mM NaCl | 6.7 | ambient | 298 | |