1BM4
MOMLV CAPSID PROTEIN MAJOR HOMOLOGY REGION PEPTIDE ANALOG
SOLUTION NMR
| NMR Experiment | ||||||||
|---|---|---|---|---|---|---|---|---|
| Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
| 1 | NOESY | 3.1 | 298 | |||||
| 2 | COSY | 3.1 | 298 | |||||
| 3 | TOCSY | 3.1 | 298 | |||||
| NMR Spectrometer Information | |||
|---|---|---|---|
| Spectrometer | Manufacturer | Model | Field Strength |
| 1 | Bruker | AMX400 | 400 |
| NMR Refinement | ||
|---|---|---|
| Method | Details | Software |
| distance geometry | REFINEMENT DETAILS CAN BE FOUND IN THE JRNL CITATION ABOVE | Discover |
| NMR Ensemble Information | |
|---|---|
| Conformer Selection Criteria | LEAST RESTRAINT VIOLATION |
| Conformers Calculated Total Number | 50 |
| Conformers Submitted Total Number | 9 |
| Additional NMR Experimental Information | |
|---|---|
| Details | THE STRUCTURE WAS DETERMINED WITH 2D-1H-NMR AND A SYNTHETIC PEPTIDE (5-7 MILLIMOLAR) |
| Computation: NMR Software | ||||
|---|---|---|---|---|
| # | Classification | Version | Software Name | Author |
| 1 | refinement | Discover | BIOSYM | |
| 2 | structure solution | BIOSYM FELIX | FELIX | |
| 3 | structure solution | FELIX ASSIGN | ASSIGN | |
| 4 | structure solution | DGII | ||
| 5 | structure solution | Discover | ||
